Filter Press Q&A

Filter Press Q&A

Here are some links to YouTube videos that better explain how a filter press works:

Basic video of a drying press: https://youtu.be/M4wBd1_CvNw

About filter cakes: https://youtu.be/aOQPr7Eomek

Recessed Plate Filter Press: https://youtu.be/JGKCpa9M0CA

470mm Press in Operation: https://youtu.be/VfalFPIFOYQ

Andritz Filter Press: https://youtu.be/8eFBoYVTLTI

 

Filter Press for Dewaxing and removal of lipids:

Q: What size presses do you sell and what size should I buy?
A:  We sell presses with plate dimensions of 470mm x 470mm, and 630mm, 800mm and larger.  A 470mm plate press can be made from 0.5 cubic feet to 4.0 cubic feet simply by adding more filter plates.  A 630mm press can be made from 2.0 to 8.0 cubic feet.  Testing should always be done on your feed material, to determine the filtration area necessary to accomplish filtration.  Just because you have a 2 foot press does not mean you will get 2 cubic feet of lipids filtered out.  This is because the cloth may blind (clog) before the plates are full.  Though testing is recommended, most customers cannot send samples to a testing lab, and lipids will change their shape once they melt.  This makes testing difficult and sometimes unreliable results are given.  We recommend getting a bigger press than needed and err on the side of caution.


Q: How much lipids can your press hold?
A: A 2 cubic foot press has an internal cavity of about 56 liters.  This means you could potentially hold 56 liters of wax.  In reality, that doesn’t work out that way as it would clog up before you reached that point.  For better filtration, we recommend a filter aide as a pre-coat.  As each application is different and all waxes, fats, and lipid ratios are different it’s difficult to know exactly how much to pre-coat.  But if we were to do a 0.5 lb per square foot pre-coat and say we introduced 19 liters of filter aid into the system, we could remove 40+ liters of lipids in one cycle.  If your crude has 15% lipids, this means you can clean 265 liters of crude per cycle (2+ hours) or 2,650 liters of 10:1 solvent : crude. This data is theoretical and will vary, but we believe it gives you a guideline.

Q: What percentage of lipids will this machine remove?
A: It will remove 98-99% of the suspended solids you run through it.  So if 98% of waxes have dropped out of suspension, then you would remove 99% of those.  In practice, that doesn’t happen since many fats and lipids remain dissolved and you need to do 2 or 3 filtrations to remove all your lipids, fats and waxes.  This has nothing to do with the function of the machine, it’s more about how these molecules behave and at what temperatures and rates they crystallize at.

Q: So you are saying you need to filter 3 times?
A: Yes and No.  If you can remove 98% of lipids with one pass and are happy with those results then congratulations, you are done.  If, because of the properties of your material, you can only remove 50% of the waxes in one pass, we recommend you winterize and filter again.

Q: Is the press capable of polishing? 
A: Yes.  Using the right filter aide, we can achieve fantastic results with a press.  A press is not like using filter paper so the results will never be as good or go down to submicron sizes. Expect to filter down to 2-5 microns with a well-used press.  If you need a fantastic polishing machine, get a filter trolley.

Q: What is polishing anyway?
A: Filtration is accomplished in three steps.  The first step, or roughing step, is where we remove the larger and heavier particles like waxes.  In a second step, we remove lighter particles like fats and lipids.  Finally, we remove very fine oils in a third pass called polishing.  As a reference roughing would be for +20 micron sizes, followed by -20 to +5 micron, finishing with a polish of -5 microns.

Q: Do you use filter paper on your press?
A: No.  Some presses do, but not this one.

Q: Does this press leak some solvent?
A: No.  Some presses do, this one does not.  This recessed plate has gaskets in every plate that ensure a leak-proof operation.

Q: How long do the gaskets and filter cloth last?
A: Gaskets should be replaced every 6 months and cloth 6-12 months

Q: Is the filter press cloth expensive?
A: It isn’t cheap, but far less expensive that using filter paper.

Q: Can I change the filter cloth every time I use the press?
A: No.  Cloth is meant to be changed once or twice a year.

Q: Do you use filter aides on this press?
A: Yes.  We have several grades and types of filter aides including food and lab grade diatomaceous earth and perlite.

Q: What is pre-coat?
A: Pre-coat is when you pump filter aid into the press before you run your solution through it.  This protects the cloth from blinding (clogging).  It’s much like when you place a bed of DE over filter paper.

Q: This press sucks, the fluid is coming out dirty as if it isn’t working!
A:  The first few minutes of filtration need to recycled back to the beginning of the process.  The filter cake is what actually does the filtration on a press.  As the press fills up, it filters better and removes smaller particles, effect is called depth filtration.

Q: How much filter surface area does your press have?
A: A 2 cubic foot press has 37.4 square feet of filtration surface area.  It has 10 plates that are 470mm x 470mm filtering on both sides of each plate. Press sizes and configurations vary.

Q: Does each plate filter finer particles as the liquid moves through the press?
A: No.  All plates filter together at the same time and filter out the same particle size, pretty much...

Q: Is this system vacuum based like a Buchner?
A: No.  It is a positive pressure system and operates up to 100 PSI.  Filtration at pressure are faster, something that cannot happen on a vacuum-based system.

Q: Will my solvent boil at 100 PSI?
A: Your solvent will boil at room temperature under vacuum.  This is not a vacuum-based system so your solvent will not boil.

Q: How large a system can I purchase?
A: We have units that can handle multiple tons of solids.

Q: What size system should I purchase?
A: How many liters/gallons of crude do you process per batch?  What percentage of wax is in your crude?  Typically, a batch takes 1-2 hours to process.

Example: 
Q: My lab does 500 liters of crude a day.  We run BHO that is 15% lipids.  Our lab runs 24/7.
A: If my batch is 100 liters, I would run 5 batches per day and do so in about 8-9 hours.  Since my crude is 15% lipids, I should remove about 15 liters of lipids per cycle.  If I intend to pre-coat, I should leave about 5 liters of space for that just in case I need that much space.  A 1 cubic foot press would hold 28 liters, which seems close to my needs.  To be safe, I can get a 2 cubic foot press allowing for future growth.  I can always make a 2 cubic foot press into any size I want by adding an end plate between plates.

Q: How does a press compare in filter surface area to your filter trolleys?
A: An 800mm filter trolley has 5.41 square feet of surface are while a 2 cubic foot press has 37.4 square feet or 691% larger.  The trolley is 14.4% the size of a 2 cubic foot press.

Q: Will the pump melt my lipids?
A: The pump does not generate heat like a centrifugal pump.

Q: Will lipids get pushed through the filter cloth?
A: No.

Q: Is this machine insulated?
A: The press is made with Polypropylene plates that have a high R value.  Your solvent will remain cold and waxes will stay solids.

Q: Is this machine food grade?
A: Yes. We make our presses with Stainless Steel and Food Grade Plastics.

Q: Is this machine FDA Certified?
A: Yes. Our presses comply with FDA Current Good Manufacturing Practices.

Q: Can these presses be used to remove carbon and clays?
A: Absolutely.  Since we filter at high pressures, removing these particles is easy with a press.

Q: How do I remove active compounds off my wax cake?
A: When you finish filtering, you can easily rinse your filter cake with cold solvent.  After the rinse, you can blow compressed air to remove solvent from the cake and clean out the press pipes.

Q: How much solvent is lost when operating this machine?
A: This is a closed system, so the loss because of evaporation should be none. Loss comes from absorption from other solids present.

Q: Do you offer automation options?
A: Yes.  We have options to close the press hydraulically on its own, and controls to do that automatically.  The press can open and close automatically, plates can open on their own and solids get shaken off and fall on a dumpster.  We also have a machine that will wash your plates with hot water automatically.

Q: How much solvent will I lose on this machine?
A: It is a sealed machine (closed loop) so no solvent will evaporate.  When you finish filtering, you blow compressed air or Nitrogen through the press to remove solvent from your solids and from the pipes.

Q: In my buchner I wash my lipids with solvent to remove remaining active compounds, can I do that with a press?
A: Yes.  Many customers wash their lipids with cold solvent after they finish filtering and thus wash out the solids.

 

Squeeze Plate Filter Press for Drying Biomass:

Many of the answers of the normal press apply to the press made for solvent removal.

Q: How exactly does this work?
A: Biomass is pumped directly from your extraction vessel into a closed system that filters out solids.  After all solids are filtered out, two inflatable bags squeeze out all solvent from the biomass.  These bags can squeeze with a pressure of almost 200 PSI. After that, compressed air is used to further dry the biomass and clear all solvent from pipes.  What is left is filtered solvent ready for solvent recovery in a ROTOVAP or FFE and a dry filter cake ready for disposal.

Q: Do I put brew bags with my plant material in the press?
A: No, biomass is pumped directly into the press.

Q: Does this system work on cold ethanol?
A: Yes it works on hot or cold solutions. This machine is incapable of operating under ultra cold temperatures. Minimum temperature is 45 F.

Q: What solvents can I use for this system?
A: Most organic solvents (ethanol, ISO, etc...) except Pentane.

Q: What pump do I use to move my biomass from my tank to the filter?
A: We supply the diaphragm pump needed.

Q: How long does the press take to dry my product?
A: Typical batch cycle times from start to finish are 1-2 hours be it for 50 pounds or 500 pounds. 

Q: How many employees does it take to operate this system?
A: One

Q: How difficult is it to operate this system?
A: Fairly straight forward.  2-3 hours of training will do.

Q: Can you send some over and help me install this and train me to use it?
A: Absolutely!

Q: How dry can this machine make the biomass.
A: It will not remove the moisture inside the cell structure.  If you start with material that will not adsorb moisture, exterior moisture can go down to 5-12% depending on how long you blow compressed air through it. The biomass gets squeezed up to 200 PSI and so removes most solvent.

Q: I have a centrifugal dryer.  How does this compare?
A: For one, there is far less manipulation of the feed material as we pump everything in.  The end product is far dryer than using a centrifugal dryer.  You will save money on labor, and you will recover more solvent and do it faster than on a centrifugal dryer. 

Q: Faster?  My centrifugal dryer does 10 pounds in 15 minutes.
A: Take into account the time you unload your extraction vessel, put your biomass in bags, load the bags to the centrifugal dryer, spin the dryer, offload the dryer and yes the overall process is faster on a press.  Remember, you need to do this 5 times on a centrifugal dryer to get the same output of a press.  Also, you will recover more solvent and loose very little solvent to evaporation on a press.  You will save on labor as well. 

Q: How is this machine better than a Delta Separations CUP15?
A: It isn’t.  The CUP is a complete system (chilling, extraction, filtration, etc...) that performs well.  Our press does not extract, only filters.  If comparing the filtration capabilities of both machines, the press is far larger; our smallest unit holds almost 200 pounds of biomass. Delta can operate at temperatures our machine cannot.

Q: I need to process 100 tons a day, can you accommodate me?
A: Yes.  We can do 50 pounds per cycle, 500 pounds per cycle, or 5 tons per cycle.  A 50 pound press can easily do 400 pounds in an 8-hour shift.

Q: Can I put whole plant in this system?
A: No.  You must debuck and grind your plant material for best results.Grind size is up to the  customer.

Q: How do I feed the plant matter into the pump?
A: The ground and debucked material is placed in an agitated extraction vessel to make a pulp of no more than 60% solids.  The more solvent used, the better the results.  The more you grind the better the results and the more biomass fits in a press.  The free flowing pulp drains into the pump which sucks at low pressure and pumps at high pressures into the press.

Q: What filter media is used, filter paper?
A: Filter cloth, which we provide the correct type for this application.

Q: How long does the cloth last?
A: 6 Months depending on care and maintenance.

Q: Do you need to use a filter aide?
A: You can.

Q: How does the equipment costs compare to competitors.
A: On a pound processing capacity basis, our smallest machine costs about $350 per pound compared to $4-5,000 per pound on our competitors.  500 pound machines cost about $200 per pound processing capability.

Q: Can I use this press to remove lipids?
A: Yes, but you shouldn’t use the squeeze function as it won’t help.  If you need to remove active ingredients from your lipids you would do a solvent rinse, not a squeeze.  Also, if you only want to dewax, then we have a press that costs half as much as these machines.